6IF8
Aeromonas hydrophila MtaN-2 complexed with adenine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-06-11 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9791 |
Spacegroup name | P 32 |
Unit cell lengths | 74.939, 74.939, 185.214 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 32.450 - 2.000 |
R-factor | 0.154 |
Rwork | 0.153 |
R-free | 0.19050 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4wkb |
RMSD bond length | 0.013 |
RMSD bond angle | 1.400 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.030 |
High resolution limit [Å] | 2.000 | 2.000 |
Rpim | 0.287 | |
Number of reflections | 76730 | 3820 |
<I/σ(I)> | 25.64 | 2.19 |
Completeness [%] | 97.7 | 93.95 |
Redundancy | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 287 | 1.5M Magnesium sulfate, 0.1M TRIS hydrochloride, pH 8.5 |