6I8X
As-p18, an extracellular fatty acid binding protein
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-11-11 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.95369 |
Spacegroup name | I 4 |
格子定数 [Å] | 102.254, 102.254, 103.392 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 14.410 - 2.300 |
R因子 | 0.181 |
Rwork | 0.179 |
R-free | 0.22000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1g74 |
結合長の平均二乗偏差(RMSD) [Å] | 0.010 |
結合角の平均二乗偏差(RMSD) [度] | 1.070 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.2) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 20.060 | 2.420 |
分解能 [Å] (高) | 2.300 | 2.300 |
Rmeas | 0.104 | 0.679 |
Rpim | 0.049 | 0.435 |
独立反射数 | 23648 | |
<I/σ(I)> | 9.8 | 1.8 |
完全性 [%] | 93.2 | 77.1 |
冗長性 | 3.7 | 1.9 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 293 | 40% ethylene glycol, 0.1 M acetate pH 4.5 |