6FLF
Deoxyguanylosuccinate synthase (DgsS) structure at 1.33 Angstrom resolution.
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-10-09 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.978570 |
Spacegroup name | C 1 2 1 |
格子定数 [Å] | 90.920, 59.480, 73.980 |
格子定数 [度] | 90.00, 102.67, 90.00 |
精密化法
残基 | 49.400 - 1.330 |
R因子 | 0.201 |
Rwork | 0.200 |
R-free | 0.22600 |
Structure solution method | MOLECULAR REPLACEMENT |
結合長の平均二乗偏差(RMSD) [Å] | 0.010 |
結合角の平均二乗偏差(RMSD) [度] | 1.040 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 49.400 | 1.410 |
分解能 [Å] (高) | 1.330 | 1.330 |
独立反射数 | 88372 | |
<I/σ(I)> | 8.4 | |
完全性 [%] | 99.2 | |
冗長性 | 4.74 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 2M NaCl 12% PEG 6K |