6AKM
Crystal structure of SLMAP-SIKE1 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-12-11 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97853 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 66.763, 66.763, 61.353 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 42.080 - 2.300 |
R-factor | 0.2074 |
Rwork | 0.204 |
R-free | 0.23800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6akk |
RMSD bond length | 0.007 |
RMSD bond angle | 0.886 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.094 | 0.821 |
Rmeas | 0.097 | 0.844 |
Rpim | 0.022 | 0.193 |
Number of reflections | 7336 | 713 |
<I/σ(I)> | 21.6 | 5.2 |
Completeness [%] | 100.0 | 100 |
Redundancy | 18.8 | 19 |
CC(1/2) | 0.948 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.1 M sodium citrate, pH 5.5; 15% (w/v) PEG 6000 |