6AAP
Crystal structure of Methanosarcina mazei PylRS(Y306A/Y384F) complexed with ZaeSeCys
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL26B2 |
Synchrotron site | SPring-8 |
Beamline | BL26B2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-11-28 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.97916 |
Spacegroup name | C 1 2 1 |
格子定数 [Å] | 100.797, 43.609, 72.478 |
格子定数 [度] | 90.00, 119.67, 90.00 |
精密化法
残基 | 37.041 - 1.500 |
R因子 | 0.1651 |
Rwork | 0.164 |
R-free | 0.19620 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2zim |
結合長の平均二乗偏差(RMSD) [Å] | 0.005 |
結合角の平均二乗偏差(RMSD) [度] | 0.948 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13_2998: ???)) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 1.530 |
分解能 [Å] (高) | 1.500 | 1.500 |
Rmeas | 0.053 | |
Rpim | 0.010 | 0.138 |
独立反射数 | 43994 | 2174 |
<I/σ(I)> | 85 | |
完全性 [%] | 99.7 | |
冗長性 | 29 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 281 | Tris-HCl (pH 8.5), PEG 200, KCl, MgCl2, sodium citrate |