6A6L
Crystal structure of the cold shock domain of YB-1 in complex with m5C RNA
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-04-04 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97930 |
Spacegroup name | P 62 |
格子定数 [Å] | 66.380, 66.380, 34.702 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 29.709 - 1.780 |
R因子 | 0.1826 |
Rwork | 0.180 |
R-free | 0.20680 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3pf5 |
結合長の平均二乗偏差(RMSD) [Å] | 0.006 |
結合角の平均二乗偏差(RMSD) [度] | 0.934 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.8.4_1496) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 30.000 | 1.840 |
分解能 [Å] (高) | 1.780 | 1.780 |
Rmerge_l_obs | 0.070 | 0.191 |
独立反射数 | 8518 | 856 |
<I/σ(I)> | 67.973 | |
完全性 [%] | 100.0 | |
冗長性 | 17.5 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 2.4M Ammonium sulfate |