6A3V
Complex structure of human 4-1BB and 4-1BBL
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-02-04 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9789 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 126.091, 137.195, 140.318 |
Unit cell angles | 90.00, 111.80, 90.00 |
Refinement procedure
Resolution | 44.666 - 3.391 |
R-factor | 0.265 |
Rwork | 0.264 |
R-free | 0.29300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5l36 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.691 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.666 | 3.520 |
High resolution limit [Å] | 3.391 | 3.400 |
Rpim | 0.121 | |
Number of reflections | 60878 | |
<I/σ(I)> | 10.7 | |
Completeness [%] | 98.8 | |
Redundancy | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.2M sodium iodide, 0.1M Bis Tris propane, pH 7.5, 20% w/v PEG 3350 |