Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-02-01 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 65.173, 74.740, 77.250 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 49.120 - 1.900 |
| R-factor | 0.1957 |
| Rwork | 0.194 |
| R-free | 0.22540 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 5lar |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.459 |
| Data reduction software | XDS |
| Data scaling software | Aimless (0.7.4) |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 49.120 | 49.120 | 1.940 |
| High resolution limit [Å] | 1.900 | 9.110 | 1.900 |
| Rmerge | 0.068 | 0.038 | 1.701 |
| Rmeas | 0.073 | 0.041 | 1.817 |
| Rpim | 0.026 | 0.016 | 0.634 |
| Total number of observations | 2200 | 15012 | |
| Number of reflections | 30122 | 334 | 1912 |
| <I/σ(I)> | 14.3 | 37.2 | 2 |
| Completeness [%] | 99.2 | 99.2 | 99 |
| Redundancy | 7.6 | 6.6 | 7.9 |
| CC(1/2) | 0.999 | 0.998 | 0.725 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.2 | 278 | 15% MMW PegSmear 0.1 M MES |
