6ZS1
Chaetomium thermophilum CuZn-superoxide dismutase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X11 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2010-04-10 |
Detector | MAR555 FLAT PANEL |
Wavelength(s) | 0.8047 |
Spacegroup name | P 61 |
Unit cell lengths | 89.110, 89.110, 310.370 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.590 - 1.560 |
R-factor | 0.1743 |
Rwork | 0.173 |
R-free | 0.20440 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1f1g |
RMSD bond length | 0.009 |
RMSD bond angle | 1.047 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.590 | 1.640 |
High resolution limit [Å] | 1.560 | 1.560 |
Rmeas | 0.008 | 0.146 |
Number of reflections | 194568 | 29651 |
<I/σ(I)> | 15 | 1.15 |
Completeness [%] | 98.0 | 92.2 |
Redundancy | 5 | 2.8 |
CC(1/2) | 0.999 | 0.416 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.2 | 289 | NaK phosphate 1.2-1.4 M |