6ZR0
Crystal structure of tetrameric fibrinogen-like recognition domain of FIBCD1 with N-acetylalanine ligand bound
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-06-30 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9795 |
Spacegroup name | P 4 |
Unit cell lengths | 119.219, 119.219, 44.180 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 84.440 - 1.940 |
R-factor | 0.19 |
Rwork | 0.189 |
R-free | 0.21000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDBID 4M7H |
RMSD bond length | 0.002 |
RMSD bond angle | 1.178 |
Data reduction software | MOSFLM |
Data scaling software | Aimless (0.5.31) |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 84.440 | 1.990 |
High resolution limit [Å] | 1.940 | 1.940 |
Rmerge | 0.080 | 0.401 |
Number of reflections | 46069 | 3105 |
<I/σ(I)> | 9.4 | |
Completeness [%] | 99.1 | 98.8 |
Redundancy | 3.2 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 1.5 M Ammonium Sulphate, 8% Dioxane, 0.1 M MES pH 6.5 |