6ZLZ
Crystal Structure of Merkel Cell Polyomavirus Virus-like Particle
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-05-25 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.976 |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 554.830, 560.990, 573.660 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 49.970 - 3.520 |
| Rwork | 0.235 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1sva |
| Data reduction software | XDS (20151231) |
| Data scaling software | XDS (20151231) |
| Phasing software | PHASER (2.6.0) |
| Refinement software | PHENIX (1.13) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 3.600 |
| High resolution limit [Å] | 3.520 | 3.520 |
| Rmeas | 0.309 | 2.883 |
| Number of reflections | 1088665 | 78618 |
| <I/σ(I)> | 9.15 | 1.06 |
| Completeness [%] | 99.8 | 98.3 |
| Redundancy | 13.5 | 12.6 |
| CC(1/2) | 0.996 | 0.332 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
