6Z8U
Copper transporter OprC
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-02-14 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.35136 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 155.113, 195.716, 165.301 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 63.140 - 2.610 |
R-factor | 0.2154 |
Rwork | 0.212 |
R-free | 0.27320 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6fok |
RMSD bond length | 0.008 |
RMSD bond angle | 1.028 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 63.140 | 2.660 |
High resolution limit [Å] | 2.610 | 2.610 |
Rpim | 0.182 | |
Number of reflections | 74873 | 7326 |
<I/σ(I)> | 5 | |
Completeness [%] | 98.0 | |
Redundancy | 13.25 | |
CC(1/2) | 0.317 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.5 M Potassium chloride 0.05 M HEPES 12-16 % v/v PEG 400 |