6YQR

BRD9 with Biphenyl-methylamino-dimethylpyridazinone

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU FR-E+ SUPERBRIGHT
Temperature [K]	100
Detector technology	CCD
Collection date	2012-10-02
Detector	RIGAKU SATURN A200
Wavelength(s)	1.541
Spacegroup name	P 1
Unit cell lengths	24.524, 33.885, 39.614
Unit cell angles	71.01, 74.35, 74.20

Refinement procedure

Resolution	27.890 - 1.684
Rwork	0.152
R-free	0.18500
Structure solution method	FOURIER SYNTHESIS
RMSD bond length	0.004
RMSD bond angle	1.172
Data reduction software	MOSFLM
Data scaling software	SCALA
Refinement software	REFMAC (5.8.0257)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	31.380	1.770
High resolution limit [Å]	1.680	1.680
Rmerge	0.020	0.035
Number of reflections	11790	1585
<I/σ(I)>	40.8	23.3
Completeness [%]	91.4	83.4
Redundancy	3.7	3.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		277	0.10M morpheus buffer 1 (1M pH 6.5), 30.00% morpheus EDO_P8K (60%) 0.10M Morpheus Amino Acids (1M)