Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | BESSY BEAMLINE 14.1 |
| Synchrotron site | BESSY |
| Beamline | 14.1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-11-04 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 0.9184 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 500.893, 500.893, 287.055 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 49.258 - 3.189 |
| R-factor | 0.2309 |
| Rwork | 0.231 |
| R-free | 0.23420 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2ms2 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | FFT |
| Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 49.258 | 49.258 | 3.380 |
| High resolution limit [Å] | 3.189 | 9.410 | 3.190 |
| Rmerge | 0.796 | 0.109 | 3.730 |
| Rmeas | 0.838 | 0.116 | 3.925 |
| Number of reflections | 680195 | 26998 | 108177 |
| <I/σ(I)> | 3.68 | 18.07 | 0.61 |
| Completeness [%] | 99.8 | 99 | 98.8 |
| Redundancy | 10.224 | 9.341 | 10.201 |
| CC(1/2) | 0.958 | 0.997 | 0.234 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 12.5% PEG 1000, 7% PEG 8000 |
