6YDG
X-ray structure of LPMO
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, DESY BEAMLINE P11 |
Synchrotron site | PETRA III, DESY |
Beamline | P11 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-09-29 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.03 |
Spacegroup name | P 41 3 2 |
Unit cell lengths | 125.670, 125.670, 125.670 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 1.900 |
R-factor | 0.22125 |
Rwork | 0.219 |
R-free | 0.26114 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5ach |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (v5.8.0230) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.950 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 27327 | 1986 |
<I/σ(I)> | 26.32 | |
Completeness [%] | 100.0 | |
Redundancy | 17.14 | |
CC(1/2) | 1.000 | 0.547 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298.15 | 3.3 M NaCl, 0.1 M citric acid pH 3.5 |