6YDE

X-ray structure of LPMO

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE MASSIF-3
Synchrotron site	ESRF
Beamline	MASSIF-3
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-04-27
Detector	DECTRIS EIGER X 4M
Wavelength(s)	0.90
Spacegroup name	P 21 21 2
Unit cell lengths	39.550, 124.370, 51.670
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.000 - 2.200
R-factor	0.19751
Rwork	0.194
R-free	0.26356
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	5ach
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	MOLREP
Refinement software	REFMAC (v5.8.0230)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.260
High resolution limit [Å]	2.200	2.200
Number of reflections	13174	977
<I/σ(I)>	5.03
Completeness [%]	96.9
Redundancy	5.41
CC(1/2)	0.982	0.620

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		289.15	0.1 M NaCl, 0.1 M Bis-Tris pH 6.5, 1.4 M (NH4)2SO4