6Y7R
Structure of Chloroflexus aggregans Cagg_3753 LOV domain C85A A56P variant (CagFbFP)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX IV BEAMLINE BioMAX |
Synchrotron site | MAX IV |
Beamline | BioMAX |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-02-08 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.976 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 54.585, 111.289, 39.220 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.250 - 1.600 |
R-factor | 0.1854 |
Rwork | 0.184 |
R-free | 0.21400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6rhf |
RMSD bond length | 0.004 |
RMSD bond angle | 1.284 |
Data reduction software | XDS |
Data scaling software | Aimless (0.7.4) |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 111.290 | 1.630 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.114 | 1.628 |
Rmeas | 0.119 | 1.694 |
Rpim | 0.033 | 0.465 |
Total number of observations | 425485 | |
Number of reflections | 32415 | 1580 |
<I/σ(I)> | 14.5 | |
Completeness [%] | 100.0 | 100 |
Redundancy | 13.1 | 13.3 |
CC(1/2) | 0.999 | 0.761 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 295 | 0.1 M Ammonium acetate, 0.1 M BIS-Tris pH 5.5, 17 % w/v PEG 10000 |