6Y5N

RING-DTC domain of Deltex1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04
Synchrotron site	Diamond
Beamline	I04
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-09-15
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	0.97950
Spacegroup name	P 21 21 21
Unit cell lengths	67.490, 86.550, 129.830
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	36.007 - 1.880
R-factor	0.1882
Rwork	0.187
R-free	0.21050
Structure solution method	SAD
RMSD bond length	0.011
RMSD bond angle	1.079
Data reduction software	DIALS
Data scaling software	autoPROC
Phasing software	SHELXCD
Refinement software	PHENIX (1.12_2829)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	36.010	1.930
High resolution limit [Å]	1.880	1.880
Rmerge	0.073	1.170
Rpim	0.048	0.530
Number of reflections	62617	4576
<I/σ(I)>	14.7	1.4
Completeness [%]	100.0	100
Redundancy	6.6	6.8
CC(1/2)	0.999	0.629

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7.6	292	BCS condition 44 (Molecular dimensions)