6Y2X

RING-DTC domains of Deltex 2, Form 2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04-1
Synchrotron site	Diamond
Beamline	I04-1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-02-24
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	0.91587
Spacegroup name	C 2 2 21
Unit cell lengths	41.756, 219.585, 120.822
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	60.411 - 1.770
R-factor	0.2437
Rwork	0.242
R-free	0.27410
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6y22
RMSD bond length	0.006
RMSD bond angle	0.841
Data reduction software	DIALS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX (1.10_2142)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	60.430	1.820
High resolution limit [Å]	1.770	1.770
Rmerge	0.052	0.770
Rpim	0.032	0.474
Number of reflections	54018	3631
<I/σ(I)>	14.4	1.8
Completeness [%]	100.0	100
Redundancy	6.6	6.8
CC(1/2)	0.999	0.581

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7.6	292	Morpheus condition 60