Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-04-20 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1.00980 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 73.686, 74.247, 97.157 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 48.626 - 1.611 |
| Rwork | 0.173 |
| R-free | 0.19760 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1zr6 |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.778 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.626 | 1.668 |
| High resolution limit [Å] | 1.611 | 1.611 |
| Number of reflections | 67366 | 5457 |
| <I/σ(I)> | 20.59 | |
| Completeness [%] | 96.8 | |
| Redundancy | 2 | |
| CC(1/2) | 1.000 | 0.698 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 293 | 0.3 M Calcium Chloride, 0.1 M Bis-Tris pH 5.7, 34% w/v PEG 3350 |
