6XV8
Crystal structure of Megabody Mb-Nb207-c7HopQ_G10
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-05-20 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 0.9763 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 79.241, 155.049, 89.754 |
Unit cell angles | 90.00, 91.73, 90.00 |
Refinement procedure
Resolution | 79.210 - 3.150 |
R-factor | 0.2566 |
Rwork | 0.255 |
R-free | 0.29660 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5lp2 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.339 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 79.230 | 3.260 |
High resolution limit [Å] | 3.150 | 3.150 |
Rmerge | 0.040 | 0.514 |
Rmeas | 0.726 | |
Number of reflections | 36041 | 3735 |
<I/σ(I)> | 7.9 | 1.3 |
Completeness [%] | 96.1 | 99.8 |
Redundancy | 1.99 | 1.99 |
CC(1/2) | 0.999 | 0.631 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 293 | 0.1 M MgCl2, 0.1 M HEPES pH 7.5, 19% PEG 4000 |