6XD4

CDC-like protein

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	AUSTRALIAN SYNCHROTRON BEAMLINE MX2
Synchrotron site	Australian Synchrotron
Beamline	MX2
Temperature [K]	100
Detector technology	CCD
Collection date	2016-08-12
Detector	ADSC QUANTUM 210
Wavelength(s)	0.9636
Spacegroup name	P 42 21 2
Unit cell lengths	121.740, 121.740, 88.910
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	43.040 - 2.100
R-factor	0.2042
Rwork	0.202
R-free	0.24670
Structure solution method	SAD
Data reduction software	XDS
Data scaling software	HKL-2000
Phasing software	SHELX
Refinement software	PHENIX (1.18.2-3874)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	20.150	2.350	2.175
High resolution limit [Å]	2.090	2.270	2.100
Rmerge	0.146
Rmeas	0.161
Rpim	0.031	0.315
Number of reflections	39801	2262	3199
<I/σ(I)>	14.8	2	1.89
Completeness [%]	97.3	72.99	100
Redundancy	14.8	22.57	15.1
CC(1/2)	0.999		0.643

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7	294	2.8 M sodium acetate
2	VAPOR DIFFUSION, HANGING DROP	7	294	2.8 M sodium acetate