6WIL
CdiB from Acinetobacter baumannii
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 22-ID |
| Synchrotron site | APS |
| Beamline | 22-ID |
| Temperature [K] | 90 |
| Detector technology | CCD |
| Collection date | 2017-06-24 |
| Detector | RAYONIX MX300-HS |
| Wavelength(s) | 1.0000 |
| Spacegroup name | P 1 |
| Unit cell lengths | 46.951, 49.283, 86.884 |
| Unit cell angles | 100.80, 90.37, 109.94 |
Refinement procedure
| Resolution | 44.007 - 2.400 |
| R-factor | 0.2105 |
| Rwork | 0.208 |
| R-free | 0.25700 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.15.2_3472) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.490 |
| High resolution limit [Å] | 2.400 | 2.400 |
| Rmerge | 0.100 | 1.300 |
| Number of reflections | 27153 | 2422 |
| <I/σ(I)> | 10.1 | 1.3 |
| Completeness [%] | 97.0 | 82.4 |
| Redundancy | 5.8 | 5.6 |
| CC(1/2) | 0.990 | 0.610 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 294 | 100mM Tris HCl pH8.0 200mM LiSU 11% PEG400 23% Ethylene glycol |
