6VN6
USP7 IN COMPLEX WITH LIGAND COMPOUND 14
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-11-11 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1.00 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 70.301, 65.680, 85.313 |
| Unit cell angles | 90.00, 94.04, 90.00 |
Refinement procedure
| Resolution | 47.900 - 2.990 |
| R-factor | 0.2212 |
| Rwork | 0.219 |
| R-free | 0.26660 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | INHOUSE MODEL |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.355 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | REFMAC |
| Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 85.100 | 3.240 |
| High resolution limit [Å] | 2.990 | 2.990 |
| Rmerge | 0.060 | 0.437 |
| Rmeas | 0.075 | 0.029 |
| Number of reflections | 15436 | 3291 |
| <I/σ(I)> | 13.9 | 2.39 |
| Completeness [%] | 97.0 | 98.2 |
| Redundancy | 2.65 | 2.7 |
| CC(1/2) | 0.998 | 0.883 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 277 | NULL |
