6VN2
USP7 IN COMPLEX WITH LIGAND COMPOUND 18
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-05-04 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.99997 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 70.044, 65.339, 85.081 |
Unit cell angles | 90.00, 93.86, 90.00 |
Refinement procedure
Resolution | 47.800 - 2.930 |
R-factor | 0.2245 |
Rwork | 0.222 |
R-free | 0.28990 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.555 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 84.890 | 3.180 |
High resolution limit [Å] | 2.930 | 2.930 |
Rmerge | 0.065 | 0.430 |
Rmeas | 0.083 | 0.050 |
Total number of observations | 37169 | |
Number of reflections | 15837 | 3429 |
<I/σ(I)> | 10.14 | 2 |
Completeness [%] | 94.7 | 95 |
Redundancy | 2.3 | 2.41 |
CC(1/2) | 0.996 | 0.895 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 277 | NULL |