6VN2
USP7 IN COMPLEX WITH LIGAND COMPOUND 18
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-05-04 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.99997 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 70.044, 65.339, 85.081 |
| Unit cell angles | 90.00, 93.86, 90.00 |
Refinement procedure
| Resolution | 47.800 - 2.930 |
| R-factor | 0.2245 |
| Rwork | 0.222 |
| R-free | 0.28990 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.555 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | REFMAC |
| Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 84.890 | 3.180 |
| High resolution limit [Å] | 2.930 | 2.930 |
| Rmerge | 0.065 | 0.430 |
| Rmeas | 0.083 | 0.050 |
| Total number of observations | 37169 | |
| Number of reflections | 15837 | 3429 |
| <I/σ(I)> | 10.14 | 2 |
| Completeness [%] | 94.7 | 95 |
| Redundancy | 2.3 | 2.41 |
| CC(1/2) | 0.996 | 0.895 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 277 | NULL |
