6VGV
Crystal structure of VidaL intein
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-08-30 |
Detector | DECTRIS PILATUS 300K |
Wavelength(s) | 1.5418 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 100.122, 40.827, 36.188 |
Unit cell angles | 90.00, 103.45, 90.00 |
Refinement procedure
Resolution | 26.950 - 1.650 |
R-factor | 0.1656 |
Rwork | 0.163 |
R-free | 0.20860 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | VidaL SeMet structure |
RMSD bond length | 0.005 |
RMSD bond angle | 0.796 |
Data reduction software | DENZO |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 26.950 | 1.750 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmeas | 0.063 | 0.323 |
Rpim | 0.023 | 0.185 |
Number of reflections | 17134 | 2567 |
<I/σ(I)> | 4 | 3.5 |
Completeness [%] | 98.9 | 94.6 |
Redundancy | 5.9 | |
CC(1/2) | 0.995 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 293 | 0.1 M sodium acetate (pH 4.6) with 2 M ammonium sulfate |