6VCO
Crystal structure of E.coli RppH in complex with ppcpA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2013-05-16 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 79.140, 38.955, 57.734 |
Unit cell angles | 90.00, 100.06, 90.00 |
Refinement procedure
Resolution | 19.480 - 1.700 |
R-factor | 0.1732 |
Rwork | 0.172 |
R-free | 0.20300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4s2y |
RMSD bond length | 0.011 |
RMSD bond angle | 1.192 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.16_3546) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.480 | 1.760 |
High resolution limit [Å] | 1.700 | 1.700 |
Number of reflections | 18406 | 1706 |
<I/σ(I)> | 24 | |
Completeness [%] | 95.3 | |
Redundancy | 7.1 | |
CC(1/2) | 0.999 | 0.923 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | 0.2 M (NH4)2SO4, 6.25% (v/v) PEG3350, and 5% (v/v) glycerol |