6VB2

HLA-B*15:02 complexed with a synthetic peptide

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CHESS BEAMLINE F1
Synchrotron site	CHESS
Beamline	F1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-12-09
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.979460
Spacegroup name	P 21 21 21
Unit cell lengths	50.849, 81.407, 110.065
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	40.155 - 1.410
R-factor	0.1992
Rwork	0.199
R-free	0.23180
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1xr8
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHENIX
Refinement software	PHENIX (1.13_2998)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.170	1.460
High resolution limit [Å]	1.360	1.400
Rmerge		0.237
Rmeas	0.043
Number of reflections	93429	9424
<I/σ(I)>	12
Completeness [%]	95.7
Redundancy	1.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		277	0.2 ammonium acetate, 0.M tri-sodium citrate dihydrate pH5.6, 30% w/v PEG4000