6UYO
Crystal structure of K37-acetylated SUMO1 in complex with PML-SIM
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-08-11 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 38.278, 38.570, 142.935 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.238 - 1.639 |
R-factor | 0.1784 |
Rwork | 0.177 |
R-free | 0.19620 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4wjo |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.14-3260_1496) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.238 | 1.698 |
High resolution limit [Å] | 1.639 | 1.639 |
Number of reflections | 25537 | 1618 |
<I/σ(I)> | 12.21 | |
Completeness [%] | 94.8 | 60.17 |
Redundancy | 4.4 | 2.9 |
CC(1/2) | 0.999 | 0.620 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 100MM SODIUM CACODYLATE PH6.5, 16% PEG3350, 10MM CALCIUM CHLORIDE |