6U3O
JR51 DQ2-p.aeru-alpha2a complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-07-01 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.95372 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 69.057, 157.650, 106.100 |
Unit cell angles | 90.00, 96.53, 90.00 |
Refinement procedure
Resolution | 47.030 - 2.743 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.030 | 2.841 |
High resolution limit [Å] | 2.743 | 2.743 |
Rpim | 0.044 | 0.374 |
Number of reflections | 58874 | 5791 |
<I/σ(I)> | 13.4 | |
Completeness [%] | 99.3 | |
Redundancy | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 23%PEG3350, 0.01mM Na-Acetate, 0.1 M Tris pH8.0 |