6U3O

JR51 DQ2-p.aeru-alpha2a complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	AUSTRALIAN SYNCHROTRON BEAMLINE MX2
Synchrotron site	Australian Synchrotron
Beamline	MX2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-07-01
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.95372
Spacegroup name	P 1 21 1
Unit cell lengths	69.057, 157.650, 106.100
Unit cell angles	90.00, 96.53, 90.00

Refinement procedure

Resolution	47.030 - 2.743
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.030	2.841
High resolution limit [Å]	2.743	2.743
Rpim	0.044	0.374
Number of reflections	58874	5791
<I/σ(I)>	13.4
Completeness [%]	99.3
Redundancy	3.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	23%PEG3350, 0.01mM Na-Acetate, 0.1 M Tris pH8.0