6TUR

human XPG, Apo1 form

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALBA BEAMLINE XALOC
Synchrotron site	ALBA
Beamline	XALOC
Temperature [K]	100
Detector technology	PIXEL
Collection date	2013-02-13
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.9786
Spacegroup name	P 21 21 21
Unit cell lengths	78.240, 89.560, 268.950
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	67.600 - 2.900
Rwork	0.237
R-free	0.28140
Structure solution method	SAD
RMSD bond length	0.007
RMSD bond angle	1.487
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	REFMAC (5.8.0258)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	134.475	3.010
High resolution limit [Å]	2.900	2.900
Number of reflections	42886	4403
<I/σ(I)>	13.1
Completeness [%]	100.0
Redundancy	80
CC(1/2)	0.998	0.528

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		295	25% PEG 3350, 100 mM Citric acid pH 3.5