6TO3
GSTF1 from Alopecurus myosuroides - covalently modified
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | BRUKER AXS MICROSTAR |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-06-01 |
| Detector | APEX II CCD |
| Wavelength(s) | 1.54 |
| Spacegroup name | P 63 2 2 |
| Unit cell lengths | 104.760, 104.760, 79.370 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 59.808 - 2.798 |
| Rwork | 0.208 |
| R-free | 0.28080 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.721 |
| Data reduction software | SAINT |
| Data scaling software | SADABS |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 59.808 | 2.860 |
| High resolution limit [Å] | 2.798 | 2.798 |
| Rmerge | 0.083 | 0.470 |
| Number of reflections | 6748 | 357 |
| <I/σ(I)> | 15.3 | |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 50.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 298 | Na/K tartrate and ammonium sulfate |
