6TL7

CRYSTAL STRUCTURE OF LECTIN-LIKE OX-LDL RECEPTOR 1 (P212121)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2009-09-24
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1.00000
Spacegroup name	P 21 21 21
Unit cell lengths	40.490, 64.700, 101.850
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	34.320 - 1.110
R-factor	0.1325
Rwork	0.132
R-free	0.16180
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1ypu
RMSD bond length	0.011
RMSD bond angle	1.249
Data reduction software	autoPROC
Data scaling software	SCALA
Refinement software	PHENIX (1.17.1_3660)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	101.850	1.170
High resolution limit [Å]	1.110	1.110
Rmerge	0.050	0.412
Rmeas	0.055	0.505
Rpim	0.055	0.282
Number of reflections	94380	7658
<I/σ(I)>	18.9
Completeness [%]	88.8
Redundancy	5.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		277	30% PEG 2000MME, 0.15M KBr, pH 6.4-7.1