6TGF
Pantoea stewartii WceF is a glycan biofilm modifying enzyme with a bacteriophage tailspike-like parallel beta-helix fold
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.2 |
Synchrotron site | BESSY |
Beamline | 14.2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-06-22 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.9184 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 100.179, 97.196, 128.949 |
Unit cell angles | 90.00, 106.40, 90.00 |
Refinement procedure
Resolution | 48.600 - 2.550 |
R-factor | 0.2283 |
Rwork | 0.227 |
R-free | 0.27250 |
Structure solution method | SAD |
RMSD bond length | 0.002 |
RMSD bond angle | 1.181 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.600 | 2.700 |
High resolution limit [Å] | 2.550 | 2.550 |
Rmeas | 0.023 | 0.128 |
Number of reflections | 74949 | 10202 |
<I/σ(I)> | 6.77 | 1.02 |
Completeness [%] | 96.4 | 81.4 |
Redundancy | 3.82 | |
CC(1/2) | 0.985 | 0.360 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 293 | 20% PEG3350, 0.2M Di-NH4-hydrogen-citrate pH 5.0 |