6TAB
Bd0314 DslA wild-type form 2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-02-12 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.92819 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 48.858, 64.670, 82.692 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.940 - 1.260 |
R-factor | 0.1518 |
Rwork | 0.150 |
R-free | 0.17670 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | EtoQ_mutant |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.31) |
Phasing software | PHASER |
Refinement software | PHENIX (1) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 64.650 | 10.000 | 1.290 |
High resolution limit [Å] | 1.260 | 5.630 | 1.260 |
Rmerge | 0.068 | 0.038 | 1.800 |
Rmeas | 0.071 | 0.039 | 1.000 |
Rpim | 0.020 | 0.011 | 0.696 |
Total number of observations | 812815 | ||
Number of reflections | 71428 | 934 | 5214 |
<I/σ(I)> | 13.2 | ||
Completeness [%] | 99.8 | 100 | 99.7 |
Redundancy | 11.4 | 11.5 | 7.6 |
CC(1/2) | 0.999 | 0.999 | 0.509 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 289 | 0.2M Lithium Sulphate 0.1M Acetate pH 4.5 30% PEG 8000 |