Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-06-30 |
| Detector | DECTRIS EIGER2 X 16M |
| Wavelength(s) | 0.9795 |
| Spacegroup name | P 1 |
| Unit cell lengths | 69.151, 103.912, 169.156 |
| Unit cell angles | 92.48, 97.34, 106.43 |
Refinement procedure
| Resolution | 66.847 - 1.910 |
| Rwork | 0.190 |
| R-free | 0.22070 |
| Structure solution method | MAD |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.401 |
| Data reduction software | xia2 |
| Data scaling software | DIALS |
| Phasing software | CRANK2 |
| Refinement software | REFMAC (5.8.0257) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 66.847 | 1.940 |
| High resolution limit [Å] | 1.910 | 1.910 |
| Number of reflections | 332768 | 16038 |
| <I/σ(I)> | 9.4 | |
| Completeness [%] | 95.9 | |
| Redundancy | 3.2 | |
| CC(1/2) | 0.997 | 0.728 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | Ammonium tartrate pH 7.0, PEG 3,350 |
