6SKA

Teneurin 2 in complex with Latrophilin 1 Lec-Olf domains

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I03
Synchrotron site	Diamond
Beamline	I03
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-04-28
Detector	DECTRIS EIGER2 X 16M
Wavelength(s)	0.97624
Spacegroup name	P 43 2 2
Unit cell lengths	96.260, 96.260, 809.220
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	52.090 - 3.860
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	xia2
Data scaling software	xia2
Phasing software	PHASER
Refinement software	BUSTER

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	202.306	4.046
High resolution limit [Å]	3.860	3.860
Number of reflections	34296	1716
<I/σ(I)>	6.187
Completeness [%]	91.2
Redundancy	12.83
CC(1/2)	0.993	0.446

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	EVAPORATION		293	0.1M potassium chloride, 0.1M HEPES pH7.5, 15% (w/v) PEG6000