6S9R
Crystal structure of SSDP from D. melanogaster
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2014-11-08 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 1.068830 |
| Spacegroup name | I 4 2 2 |
| Unit cell lengths | 137.503, 137.503, 53.863 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 43.480 - 2.400 |
| R-factor | 0.2267 |
| Rwork | 0.225 |
| R-free | 0.26530 |
| Structure solution method | SAD |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.923 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | SHELXCD |
| Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 43.480 | 2.486 |
| High resolution limit [Å] | 2.400 | 2.400 |
| Rmerge | 0.053 | |
| Rmeas | 0.055 | |
| Rpim | 0.011 | |
| Number of reflections | 10414 | 1010 |
| <I/σ(I)> | 33.38 | |
| Completeness [%] | 99.5 | |
| Redundancy | 25.4 | |
| CC(1/2) | 1.000 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 298 | 0.1 M MES, 1.7-1.9 M Ammonium Sulfate 0.01 M MgCl2 |
