6RZ2
SalL with Chloroadenosine
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 120 |
| Detector technology | PIXEL |
| Collection date | 2018-11-24 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.976230 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 50.842, 111.579, 165.565 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 49.470 - 1.770 |
| R-factor | 0.17219 |
| Rwork | 0.171 |
| R-free | 0.20148 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2q6i |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.673 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.470 | 1.800 |
| High resolution limit [Å] | 1.770 | 1.770 |
| Rmerge | 0.080 | 0.780 |
| Rpim | 0.050 | 0.430 |
| Number of reflections | 92806 | 4561 |
| <I/σ(I)> | 15.7 | 2.6 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 8 | 8.2 |
| CC(1/2) | 0.990 | 0.830 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 298 | 0.1 M HEPES pH 7; 20% PEG 6000; 0.2 M CaCl2 |
