6RW7
An AA10 LPMO from the shipworm symbiont Teredinibacter turnerae
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-04-23 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9795 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 36.644, 62.516, 43.185 |
Unit cell angles | 90.00, 99.13, 90.00 |
Refinement procedure
Resolution | 35.250 - 1.400 |
R-factor | 0.1537 |
Rwork | 0.152 |
R-free | 0.17510 |
Structure solution method | SAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.565 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | CRANK2 |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.180 | 1.420 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.072 | 0.796 |
Rmeas | 0.083 | 0.972 |
Rpim | 0.041 | 0.548 |
Number of reflections | 37737 | 4927 |
<I/σ(I)> | 12.3 | 1.3 |
Completeness [%] | 99.5 | 95.6 |
Redundancy | 3.9 | 2.7 |
CC(1/2) | 0.998 | 0.606 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 292 | 0.2 M magnesium formate dehydrate pH 7.0 and 20 % w/v PEG 3350 |