6RIS

The Kb42S variant of the molybdenum storage protein

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X10SA
Synchrotron site	SLS
Beamline	X10SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2015-11-30
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1.738
Spacegroup name	P 63 2 2
Unit cell lengths	116.390, 116.390, 237.220
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	49.298 - 2.100
R-factor	0.1885
Rwork	0.187
R-free	0.21300
Structure solution method	FOURIER SYNTHESIS
Starting model (for MR)	4ndo
RMSD bond length	0.004
RMSD bond angle	0.774
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHENIX
Refinement software	PHENIX ((1.14_3260: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.200
High resolution limit [Å]	2.100	2.100
Number of reflections	104313	13361
<I/σ(I)>	13.4
Completeness [%]	99.4
Redundancy	8.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	5.6	293	0.1 M Na-citrate, pH 5.6, 1 M ammonium phosphate, 20% glycerol