6RCD
Octamer C-Domain P140 Mycoplasma genitalium.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALBA BEAMLINE XALOC |
| Synchrotron site | ALBA |
| Beamline | XALOC |
| Temperature [K] | 80 |
| Detector technology | PIXEL |
| Collection date | 2017-06-27 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1.07216 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 114.509, 83.020, 118.160 |
| Unit cell angles | 90.00, 117.50, 90.00 |
Refinement procedure
| Resolution | 52.410 - 1.980 |
| R-factor | 0.178 |
| Rwork | 0.176 |
| R-free | 0.20600 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6rcc |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.040 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.10.3) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 52.410 | 2.090 |
| High resolution limit [Å] | 1.980 | 1.980 |
| Number of reflections | 67417 | 9766 |
| <I/σ(I)> | 10.5 | |
| Completeness [%] | 98.5 | |
| Redundancy | 3.4 | |
| CC(1/2) | 0.998 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293.15 | DL-Malic acid and Bis-Tris propane |
