6R4I
Crystal structure of human GFAT-1 G461E
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE MASSIF-3 |
Synchrotron site | ESRF |
Beamline | MASSIF-3 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-05-12 |
Detector | DECTRIS EIGER X 4M |
Wavelength(s) | 0.97 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 152.753, 152.753, 165.988 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.679 - 2.586 |
R-factor | 0.1925 |
Rwork | 0.192 |
R-free | 0.21890 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6r4e |
RMSD bond length | 0.002 |
RMSD bond angle | 0.444 |
Data reduction software | XDS (Jan 26, 2018) |
Data scaling software | XDS (Jan 26, 2018) |
Phasing software | PHENIX ((dev_2499: ???)) |
Refinement software | PHENIX ((dev_2499: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.680 | 2.680 |
High resolution limit [Å] | 2.586 | 2.586 |
Number of reflections | 61581 | 5916 |
<I/σ(I)> | 17.49 | |
Completeness [%] | 99.6 | |
Redundancy | 10 | |
CC(1/2) | 0.999 | 0.556 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 0.1 M Bis tris propane pH 8.5, 0.35 M Potassium sodium tartrate, 20 % PEG3350 |