6R4H
Crystal structure of human GFAT-1 G451E
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2018-04-26 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1.0 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 154.073, 154.073, 162.926 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.982 - 2.244 |
R-factor | 0.1866 |
Rwork | 0.186 |
R-free | 0.20340 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6r4e |
RMSD bond length | 0.003 |
RMSD bond angle | 0.535 |
Data reduction software | XDS (Jan 26, 2018) |
Data scaling software | XDS (Jan 26, 2018) |
Phasing software | PHENIX ((dev_2499: ???)) |
Refinement software | PHENIX ((dev_2499: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.982 | 2.320 |
High resolution limit [Å] | 2.240 | 2.240 |
Number of reflections | 93589 | 9028 |
<I/σ(I)> | 16.87 | |
Completeness [%] | 99.7 | |
Redundancy | 7.4 | |
CC(1/2) | 0.999 | 0.627 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 0.1 M Bis tris propane pH 8.25, 0.4 M Potassium sodium tartrate, 20 % PEG3350 |