6R46
Crystal structure of LPOR (Thermosynechococcus elongatus) complexed with NADP+ at 2.5A resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-10-01 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97776 |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 134.950, 134.950, 104.750 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 78.000 - 2.500 |
R-factor | 0.198 |
Rwork | 0.196 |
R-free | 0.24900 |
Structure solution method | SAD |
RMSD bond length | 0.013 |
RMSD bond angle | 1.600 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0189) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 78.000 | 2.600 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.082 | 0.713 |
Number of reflections | 20005 | 20005 |
<I/σ(I)> | 14.4 | 2.1 |
Completeness [%] | 100.0 | 99.9 |
Redundancy | 8.6 | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 293 | 10MM ZNSO4,0.2M LI3CITRATE, 30% PEG3350 |