Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 77 |
| Detector technology | CCD |
| Collection date | 2016-09-17 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.97895 |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 109.690, 152.690, 176.230 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 57.700 - 2.520 |
| R-factor | 0.19082 |
| Rwork | 0.189 |
| R-free | 0.22352 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6r3t |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.901 |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | PHENIX |
| Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 57.700 | 2.560 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Number of reflections | 50406 | 3692 |
| <I/σ(I)> | 18.9 | |
| Completeness [%] | 98.4 | |
| Redundancy | 4.3 | |
| CC(1/2) | 0.999 | 0.760 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 21% PEG 3350, 0.2M Tri-potassium citrate |
