Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALBA BEAMLINE XALOC |
| Synchrotron site | ALBA |
| Beamline | XALOC |
| Temperature [K] | 77 |
| Detector technology | PIXEL |
| Collection date | 2016-11-25 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.989 |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 110.026, 151.569, 176.548 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 115.000 - 2.210 |
| R-factor | 0.19106 |
| Rwork | 0.190 |
| R-free | 0.21568 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6r3t |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.809 |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | PHENIX |
| Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 115.000 | 2.330 |
| High resolution limit [Å] | 2.210 | 2.210 |
| Number of reflections | 73757 | 10661 |
| <I/σ(I)> | 20.6 | |
| Completeness [%] | 99.8 | |
| Redundancy | 4.8 | |
| CC(1/2) | 0.997 | 0.516 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 19 % PEG3350, 0.2M Tri-potassium citrate |
