Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALBA BEAMLINE XALOC |
| Synchrotron site | ALBA |
| Beamline | XALOC |
| Temperature [K] | 293 |
| Detector technology | PIXEL |
| Collection date | 2016-03-10 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1.12712 |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 109.600, 152.940, 172.710 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 54.860 - 2.730 |
| R-factor | 0.17836 |
| Rwork | 0.176 |
| R-free | 0.22470 |
| Structure solution method | SAD |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.932 |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | PHENIX |
| Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 62.000 | 2.770 |
| High resolution limit [Å] | 2.700 | 2.700 |
| Rmerge | 0.047 | |
| Rpim | 0.052 | |
| Number of reflections | 39641 | 39641 |
| <I/σ(I)> | 19.1 | |
| Completeness [%] | 98.9 | |
| Redundancy | 4.6 | 4.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 11% PEG 8000 0.1M Imidazole pH 8 0.2M Calcium acetate |
