6QZU
Getah virus macro domain
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-02-11 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.91976 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 46.552, 71.358, 94.954 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 41.800 - 2.000 |
| R-factor | 0.196 |
| Rwork | 0.194 |
| R-free | 0.23108 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3gpg |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.304 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 41.800 | 2.050 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.134 | 0.748 |
| Rmeas | 0.173 | 0.976 |
| Rpim | 0.108 | 0.619 |
| Number of reflections | 22033 | 6918 |
| <I/σ(I)> | 7.3 | 2.1 |
| Completeness [%] | 99.8 | 99.8 |
| Redundancy | 4.5 | 4.3 |
| CC(1/2) | 0.989 | 0.603 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 6 | 293 | 0,2M Imidazole Malate pH6 30% PEG 4K |
