Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-07-04 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 0.97265 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 184.017, 184.017, 87.285 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 92.008 - 3.090 |
| Rwork | 0.183 |
| R-free | 0.22590 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1dlh |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.681 |
| Data reduction software | xia2 |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 92.020 | 3.170 |
| High resolution limit [Å] | 3.086 | 3.086 |
| Rmerge | 0.191 | 3.078 |
| Rmeas | 0.201 | 3.231 |
| Rpim | 0.060 | 0.979 |
| Number of reflections | 31506 | 2293 |
| <I/σ(I)> | 10.3 | |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 11 | 10.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 6 | 291 | Seeded with DR1-QAR crystals. 0.2M LiCl, 20% PEG 6K, 0.1M MES |
